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Mono Sodium Phosphate monohydrate is manufactured by method using either phosphate rock or dicalcium phosphate or any similar phosphatic material as a base material from which the mono-sodium phosphate is produced. For example, as a steam coil, in order that the mixture may be warmed to facilitate the reaction. After the completion of the above reaction the calcium sulphate is removed by filtration and washed with water until entirely free from mono-calcium phosphate.